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1 article(s) from Taya, Akihito

Deoxyfluorination of acyl fluorides to trifluoromethyl compounds by FLUOLEAD^®/Olah’s reagent under solvent-free conditions

Yumeng Liang,
Akihito Taya,
Zhengyu Zhao,
Norimichi Saito and
Norio Shibata

Beilstein J. Org. Chem. 2020, 16, 3052–3058, doi:10.3762/bjoc.16.254

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Graphical Abstract

Figure 1: Ratios of CF₃-containing drugs in marketed fluoro-pharmaceuticals and registered fluoro-agrochemica...

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Figure 2: Selected examples of CF₃-containing biologically active molecules.

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Scheme 1: Transformation of acyl fluorides to trifluoromethyl compounds. a) Deoxyfluorination of acyl fluorid...

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Scheme 2: The substrate scope of acyl fluorides. Reaction conditions: 1 (0.3 mmol), FLUOLEAD^® (0.9 mmol, 3.0 ...

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Scheme 3: Mechanism of deoxyfluorination of acyl fluorides 1 with FLUOLEAD^®/Olah’s reagent to trifluoromethyl...

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Letter

Published 14 Dec 2020

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Deoxyfluorination of acyl fluorides to trifluoromethyl compounds by FLUOLEAD®/Olah’s reagent under solvent-free conditions

Deoxyfluorination of acyl fluorides to trifluoromethyl compounds by FLUOLEAD^®/Olah’s reagent under solvent-free conditions